4-Nitrophenyl 1-naphthoate

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4-Nitro­phenyl 1-naphthoate

In the title compound, C(17)H(11)NO(4), the dihedral angle between the two benzene rings is 8.66 (3)°. The nitro group is twisted by 4.51 (9)° out of the plane of the aromatic ring to which it is attached. The presence of inter-molecular C-H⋯O contacts in the crystal structure leads to the formation of chains along the c axis.

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Methyl 1-bromo-2-naphthoate

In the mol-ecular structure of the title compound, C(12)H(9)BrO(2), the methoxy-carbonyl group is twisted by a dihedral angle of 29.8 (3)°with respect to the naphthalene ring system. An overlapped arrangement is observed between parallel naphthalene ring systems of adjacent mol-ecules, and the face-to-face distance of 3.590 (9) Å suggests there is π-π stacking in the crystal structure.

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Ammonium 1-hydr­oxy-2-naphthoate

The title compound, NH(4) (+)·C(11)H(7)O(3) (-), was obtained by slow evaporation of a 30% ammonia solution of 1-hydr-oxy-2-naphthoic acid. The crystal structure is stabilized by inter-molecular N-H⋯O hydrogen bonds, forming layers parallel to the bc plane.

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(4-Chlorobenzoyl)(4-chlorophenyl)amino 3-(2-nitrophenyl)propanoate

In the title hydroxamic acid derivate, C22H16Cl2N2O5, the nitro-substituted benzene ring forms dihedral angles of 14.11 (15) and 16.08 (15)°, with the 4-chloro-benzoyl and 4-chloro-phenyl benzene rings, respectively. The dihedral angle between the chloro-substituted benzene rings is 2.28 (13)°. In the crystal, mol-ecules are linked by weak C-H⋯O hydrogen bonds, forming chains along [100].

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Synthesis and antimicrobial activity of some 1-(2,4-dinitrophenyl)-3-(3-nitrophenyl)-5-(4-substituted phenyl)-4-bromo-2-pyrazolines and 1-(2,4-dinitrophenyl)-3-(3-nitrophenyl)-5-(4-substituted phenyl)-2-pyrazolin-4-ones.

A series of 1-(2,4-dinitrophenyl)-3-(3-nitrophenyl)-5-(4-substituted phenyl)-2-pyrazolin-4-ones (4a-e) have been synthesized by the oxidation of 1-(2,4-dinitrophenyl)-3-(3-nitrophenyl)-5-(4-substituted phenyl)-4-bromo-2-pyrazolines (3a-e) with dimethylsulfoxide. The structure has been established on the basis of spectral data (IR,1H NMR). The synthesized compounds have been screened in vitro fo...

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ژورنال

عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online

سال: 2010

ISSN: 1600-5368

DOI: 10.1107/s1600536810011736